Sunday, April 3, 2016

Separations

Today I'm going to be discussing a little topic that is extremely important in chemical engineering and that is separations. Separations is basically exactly what the name implies but it goes into massive depth in the field of chemical engineering. I personally am taking a class right now that just serve as an intro into separations and it's extremely difficult and complicated already. On the most basic level, separation processes are processes by which things are separated from other things. Now that seems pretty redundant and almost meaningless so let’s get a bit more specific. A few weeks ago, I talked about distillation. Distillation is a specific type of separation and there are even many subsections of distillation that are further divided into more specific types of distillation (tray, flash, etc. and there are even subdivisions of these types honestly).
So we’ve got one example of separations. But what other kinds are there out there? Let’s go with something simple and then expand it a bit to an industry example: filters. Filters are everywhere around you. They’re in the air intake vents in your house or apartment, on your AC unit, in your fridge, in your Brita, everywhere. Basically, filters are a way of separating things based on the size of the particles involved. You could separate rocks from water with a towel, or cheese from whey with cheesecloth and you’d be filtering in each case. Now let’s look at a specific industry example of filtration. You may have heard of reverse osmosis from somewhere or another. It’s a filtration process that relies on specific membranes through which water molecules (and anything smaller) can pass through unhindered while bigger particles (dirt, salt, or metals) cannot. Reverse osmosis is extremely useful in regions that don’t have access to freshwater because it can turn saltwater into drinkable water. Now there are major downsides to reverse osmosis – it is extremely energy intense and thus is really only optimal for places without access to freshwater from other sources. That is not to say that it’s not an incredibly powerful separation method though. For most of human history, the only way to separate salt from water was to evaporate it and re-condense the evaporated water in another container. This is time consuming and very difficult. Reverse osmosis is continuous and freshwater can be continually generated as the process goes. See the below picture for a very basic diagram of this process. It’s just like any other filtration. You’re relying on the fact that smaller particles will fit through smaller holes while larger ones will not. Now filtration can be a little more complicated a times – filters can also rely on differences in chemical or electric properties to remove impurities rather than just pores.
Filtration is just one example of separations though. The field is quite possibly endless and that’s why I’m going to try to go into just some of the biggest ones here and give enough depth to show why they’re each important. Let’s move on to absorption and stripping (not that kind of stripping). Absorption and stripping are extremely common methods for liquid-liquid, liquid-gas, or gas-gas separations. The idea is that two streams can be passed by one another where one stream contains a contaminant that we want to remove and the other stream will be pure but used to absorb some of the unwanted material. So say we have some methanol vapor (very bad stuff to consume) contamination in an air sample and we want to remove it so that we can use the air for medical purposes. We could use a water stream running counter-current (in the opposite direction) of the gas stream in a separation unit to pull out the methanol and purify the air so that it’s safe to use. The methanol gets caught up in the water much more easily than it does in the air and so as the streams pass one another, methanol is pulled into the liquid, while the air stream is purified and passes through the other side. The methanol is now in the liquid phase and though methanol-water is very hard to separate, it is much less dangerous in its liquid form than its vapor form. You still shouldn’t drink it though. Methanol is extremely dangerous and can cause you go to blind in even very small amounts. It has its uses though. Methanol-water (the mixture of the two) is a very good solvent and is often used in analytical chemistry.
In industry, separations are easily the most important part of any chemical production processes. In any process, there are unwanted byproducts and contaminants that must be removed before they can be taken to market. If you ever drive past a refinery, the tallest towers you see are the separation towers and they’re the most expensive component on-site because they’re extremely important. You can’t sell your gasoline if it has water in it or you’re oxygen if it’s contaminated with borane gas. You have to separate out the unwanted components. Now you can never truly get pure separations (100% of one thing). There will always be some small contaminants. That’s why you shouldn’t freak out when you hear there’s arsenic in the water. There’s arsenic in all water but in your drinking water, the amounts are generally of no concern. There can be cases where the contaminants exceed acceptable levels and then separations must be done. Look at Flint, Michigan for example. Due to improper handling with the switch over from Detroit’s water supply to lake water, the acidity of the lake water caused corrosion in the old lead pipes and now lead has been seeded into the water supply. To remove this lead, you need a high grade filter specifically designed for heavy metal filtration. I should also point out that again, having a tiny amount of lead in the water is not dangerous. All water around the world contains some small amount of lead but the amounts are generally so small as to be no concern (I’m talking about parts per trillion, and not parts per million – PPM is generally a common measure for the amount of contaminant in something). All that said, being able to separate contaminants from the target product is extremely important not only to big companies but also to individuals.
There are easily hundreds of different types of separations and I’ve only just gone over a few of them today. Many of them are very complicated and a bit hard to explain in layman’s terms. For example if you really want to go down the rabbit hole for separations, lookup “tray hydraulic distillation” or “packed tower” for some really dry and technical (though extremely meaningful) reading. For most of us, we would never even use the word separation processes to describe the kinds of things we do that might fit under that heading. We filter stuff, we boil off stuff, we absorb stuff, but all of those things fall into the field of separations. Almost ever drink you’ve ever had was probably separated somewhere in the production line. Fruit juices are separated from pulp via filtration. Salt can be separated from salt water via boiling to make sea salt and if you re-condense the air, pure drinking water. I’ve included some interesting links below that the kids might want to check out if you want to try some basic separations experiments at home. I hope I’ve done an acceptable job of introducing the field of separations to you guys. If you have any questions or want to see a specific topic, post it in the comments and I’ll talk about it next time.

http://www.rsc.org/learn-chemistry/resource/res00000386/separating-sand-and-salt?cmpid=CMP00005908


Image source
http://puretecwater.com/what-is-reverse-osmosis.html




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